XVI.—The condensation of ethyl acetoacetate with p-dimethylaminobenzaldehyde and ammonia
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Spectrophotometric Determination of Hydralazine Using p-Dimethylaminobenzaldehyde
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The mechanism of the TiCl4-promoted condensation of methyl acetoacetate, isobutyraldehyde, and indole was studied by a combination of theoretical and experimental techniques. The energy profile of plausible reaction paths was evaluated by DFT calculations, and various reaction intermediates were isolated or observed in solution by NMR spectroscopy. Theoretical and experimental results indicate ...
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ژورنال
عنوان ژورنال: J. Chem. Soc., Trans.
سال: 1920
ISSN: 0368-1645
DOI: 10.1039/ct9201700137